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NEW seaFAST - Automated ICPMS Preconcentration System for Undiluted Seawater
The seaFAST is an
automated on-line ICPMS sample introduction system for the determination of ultra trace metals in
undiluted seawater. The seaFAST system improves detection limits for a range of elements through preconcentration, matrix elimination, and reduced procedural blanks.
seaFAST is a complete system that incorporates two high-purity injection valves. The system takes up an aliquot of sample in a loop on one inert injection valve and preconcentrates
elements such as Ti, Co, Ni, Cu, Zn, Cd, and Pb on a chelation column attached to a second high-purity valve. The column chemistry allows Na, Cl, Mg, and Ca matrix ions to pass through. The concentrated metals are then eluted into a nebulizer and detected using an ICPMS instrument.
The seaFAST system also preconcentrates the following elements: Al, Sc, V, Mn, Fe, Ga, Y, Zr, Nb, Mo, Pd, Ag, In, Sn, La, Ce, Pr, Nd, Sm, Eu, Gd, Tb, Ho, Er, Tm, Yb, Lu, Hf, Ta, W, Re, Os, Ir, Pt, Bi, Th, and U.
The seaFAST system provides many benefits, including:
• Automated Matrix Removal and Analyte Preconcentration - Low and sub-ppt detection limits in undiluted seawater.
• Low Procedural Blanks - Elimination of dilution steps avoids contamination from the diluent, acid, secondary vessels, and laboratory handling. Concentrations as analyzed are up to 10x higher than with dilution methods, improving S/N.
• Fast Turn Around - On-line automated preconcentration and matrix elimination reduces lengthy and contamination-prone manual sample preparation steps and allows for better control and correction of procedural and instrumental blanks.
• Alternate Chemistries - seaFAST system can be used with many column chemistries and mixed chemistries designed to target single or oligo element preconcentration and determination in seawater.
All seaFAST systems include:
• SC Autosampler with FAST PC3 Complete
• 6 Channel precision MP2 micro peristaltic pump
• High-purity fluoropolymer injection valves and all connections
• seaFAST column with all PFA construction and PTFE frits
• Trace metals cleanup column (2 ea)
• Suggested methods
seaFAST Options
seaFAST 1
Preconcentration Mode: A chelation column binds transition metals and rare earth elements but allows matrix Na+, Cl-, Ca2+, ad Mg2+ ions to be rinsed out. After the preconcentration step, analytes are eluted and detected by ICPMS. (2 valves)
seaFAST 2
Preconcentration and Direct Modes: The capabilities of seaFAST 1, plus online dilution with internal standard during the same analytical run. (3 valves)
seaFAST3
Preconcentration, Direct and Hydride Modes: The capabilities of seaFAST 2, plus simultaneous batch-modes hydride generation for As, Se and other hydride forming elemets. (5 valves, 2 syringes)
All seaFAST systems may be configured to operate as high throughput SC-FAST systems for direct sample analysis.
Download seaFAST flier for information
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seaFAST Multi-Mode Element Chart |
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seaFAST 1 System Diagram |
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Standard mode ICPMS calibration of Cu in seawater. seaFAST eliminates the
NaAr+on 63Cu+ |
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Spike Recoveries Shown From
ppt-level Spikes in NASS-5 Seawater |
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| Method Detection Limits for a Normal Laboratory Environment |
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